Precursor driven one pot synthesis of wurtzite and chalcopyrite CuFeS2.

نویسندگان

  • Prashant Kumar
  • Sitharaman Uma
  • Rajamani Nagarajan
چکیده

A facile precursor dependent single step, one pot solution based synthesis of wurtzite and chalcopyrite polymorphs of CuFeS2 has been developed by reacting a Cu(I) thiourea complex with Fe2(SO4)3 and FeCl3 separately in ethylene glycol. The phases have been characterized by structural refinements, SEM-EDX, TEM-SAED, Raman, UV-Visible spectroscopy and TGA measurements.

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عنوان ژورنال:
  • Chemical communications

دوره 49 66  شماره 

صفحات  -

تاریخ انتشار 2013